Synthesis and crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate
Identifieur interne : 000933 ( Main/Exploration ); précédent : 000932; suivant : 000934Synthesis and crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate
Auteurs : M. Belhouchet [Tunisie, France] ; T. Mhiri [Tunisie]Source :
- Crystallography Reports [ 1063-7745 ] ; 2013-01-01.
Abstract
Abstract: The crystal structure of 3-ammonium-4-hydroxyphenyl sulfonate hemihydrate C6H3(NH3)(OH)SO3 · 0.5H2O is determined by single-crystal X-ray diffraction. The unit cell parameters are as follows: a = 11.2395(3), b = 10.3814(3), c = 13.7509(4) Å, β = 100.326(1)°, V = 1578.49(8) Å3, space group P21/n, Z = 4. The crystal structure can be described us a succession of infinite corrugated layers parallel to ab plane. These layers consist of rings formed by four sulfonate molecules located around a center of symmetry. The rings are connected to each other and to water molecules via O-H...O hydrogen bonds. The structure is further stabilized by π-π interactions between phenyl rings of organic entities of successive layers.
Url:
DOI: 10.1134/S106377451301015X
Affiliations:
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